JPS6328415B2 - - Google Patents
Info
- Publication number
- JPS6328415B2 JPS6328415B2 JP9175684A JP9175684A JPS6328415B2 JP S6328415 B2 JPS6328415 B2 JP S6328415B2 JP 9175684 A JP9175684 A JP 9175684A JP 9175684 A JP9175684 A JP 9175684A JP S6328415 B2 JPS6328415 B2 JP S6328415B2
- Authority
- JP
- Japan
- Prior art keywords
- water
- allyl alcohol
- allyl
- composition
- phase
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- XXROGKLTLUQVRX-UHFFFAOYSA-N allyl alcohol Chemical compound OCC=C XXROGKLTLUQVRX-UHFFFAOYSA-N 0.000 claims description 56
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 41
- 239000000203 mixture Substances 0.000 claims description 36
- HVAMZGADVCBITI-UHFFFAOYSA-M pent-4-enoate Chemical compound [O-]C(=O)CCC=C HVAMZGADVCBITI-UHFFFAOYSA-M 0.000 claims description 17
- 238000010992 reflux Methods 0.000 claims description 15
- 238000000034 method Methods 0.000 claims description 11
- 239000008346 aqueous phase Substances 0.000 claims description 7
- 238000004821 distillation Methods 0.000 claims description 7
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 3
- 239000007791 liquid phase Substances 0.000 claims description 2
- 238000009833 condensation Methods 0.000 claims 1
- 230000005494 condensation Effects 0.000 claims 1
- 239000012071 phase Substances 0.000 description 31
- 239000007788 liquid Substances 0.000 description 8
- 239000002994 raw material Substances 0.000 description 7
- 238000009835 boiling Methods 0.000 description 5
- 238000000605 extraction Methods 0.000 description 5
- 238000010586 diagram Methods 0.000 description 4
- 230000018044 dehydration Effects 0.000 description 3
- 238000006297 dehydration reaction Methods 0.000 description 3
- 239000003795 chemical substances by application Substances 0.000 description 2
- 238000001816 cooling Methods 0.000 description 2
- 238000001704 evaporation Methods 0.000 description 2
- 230000008020 evaporation Effects 0.000 description 2
- 125000003903 2-propenyl group Chemical group [H]C([*])([H])C([H])=C([H])[H] 0.000 description 1
- 238000005191 phase separation Methods 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 239000011541 reaction mixture Substances 0.000 description 1
- 238000011084 recovery Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP9175684A JPS60237032A (ja) | 1984-05-10 | 1984-05-10 | アリルアルコ−ルの精製方法 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP9175684A JPS60237032A (ja) | 1984-05-10 | 1984-05-10 | アリルアルコ−ルの精製方法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS60237032A JPS60237032A (ja) | 1985-11-25 |
| JPS6328415B2 true JPS6328415B2 (en]) | 1988-06-08 |
Family
ID=14035380
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP9175684A Granted JPS60237032A (ja) | 1984-05-10 | 1984-05-10 | アリルアルコ−ルの精製方法 |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS60237032A (en]) |
Families Citing this family (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP3585989B2 (ja) * | 1995-03-29 | 2004-11-10 | 大阪有機化学工業株式会社 | アクリル酸メチルまたはメタクリル酸メチルとメタノールの分離方法 |
| JP5094148B2 (ja) * | 2006-02-02 | 2012-12-12 | 昭和電工株式会社 | アリルアルコールの製造方法 |
| SA07280020B1 (ar) * | 2006-02-02 | 2011-04-24 | شوا دينكو كيه. كيه. | طريقة تقطير ازيوتروبية |
| TWI518059B (zh) | 2013-06-05 | 2016-01-21 | 大連化學工業股份有限公司 | 丙烯醇之製造方法 |
| SG11201802755WA (en) * | 2015-10-14 | 2018-05-30 | Dow Global Technologies Llc | Process for purification of methyl methacrylate |
| CN107501047A (zh) * | 2017-09-07 | 2017-12-22 | 太原理工大学 | 一种制备高纯度丙烯醇的方法 |
| CN107698428B (zh) * | 2017-09-27 | 2022-09-20 | 湖北绿色家园材料技术股份有限公司 | 一种分离烯丙醇中水分的方法 |
-
1984
- 1984-05-10 JP JP9175684A patent/JPS60237032A/ja active Granted
Also Published As
| Publication number | Publication date |
|---|---|
| JPS60237032A (ja) | 1985-11-25 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| EXPY | Cancellation because of completion of term |